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Submonomer synthesis of peptoids containing trans -inducing N -imino- and N -alkylamino-glycines

https://doi.org/10.1039/d1sc00717c

Davern, Carolynn M. ; Lowe, Brandon D. ; Rosfi, Adam ; Ison, Elon A. ; Proulx, Caroline ( June 2021 , Chemical Science)

The use of hydrazones as a new type of submonomer in peptoid synthesis is described, giving access to peptoid monomers that are structure-inducing. A wide range of hydrazones were found to readily react with α-bromoamides in routine solid phase peptoid submonomer synthesis. Conditions to promote a one-pot cleavage of the peptoid from the resin and reduction to the corresponding N -alkylamino side chains were also identified, and both the N -imino- and N -alkylamino glycine residues were found to favor the trans -amide bond geometry by NMR, X-ray crystallography, and computational analyses.
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Expert Algorithm for Substance Identification Using Mass Spectrometry: Statistical Foundations in Unimolecular Reaction Rate Theory

https://doi.org/10.1021/jasms.3c00089

Jackson, Glen P. ; Mehnert, Samantha A. ; Davidson, J. Tyler ; Lowe, Brandon D. ; Ruiz, Emily A. ; King, Jacob R. ( May 2023 , Journal of the American Society for Mass Spectrometry)
Expert Algorithm for Substance Identification Using Mass Spectrometry: Application to the Identification of Cocaine on Different Instruments Using Binary Classification Models

https://doi.org/10.1021/jasms.3c00090

Mehnert, Samantha A. ; Davidson, J. Tyler ; Adeoye, Alexandra ; Lowe, Brandon D. ; Ruiz, Emily A. ; King, Jacob R. ; Jackson, Glen P. ( May 2023 , Journal of the American Society for Mass Spectrometry)